Liquid/amorphous structure measurement -------------------------------------- A python program 'multiangle.py' is available for automatic data acquisition of EDXD pattern with varying 2θ angle. - Open the python program by running 'multiangle.bat' from the desktop shortcut. .. figure:: /images/operation/multiangle_setup.png :alt: multiangle_setup :width: 720px :align: center You have the following 3 options: 1. Create a new setup automatically by clicking Setup in main window. In the pop-up window enter desired q-range and usable E range, and % overlap for the measurements. The built in algorithm will calculate optimal 2theta angles and populate the main window. .. figure:: /images/operation/multiangle_automatic.png :alt: multiangle_automatic :width: 320px :align: center 2. Load previously saved setup, click :guilabel:`Load` in main window 3. Add 2-theta angles manually by clicking :guilabel:`Add` in the main window for each angle. Adjust the slit sizes and exposure times for each 2-theta .. csv-table:: Input paramters description :header: "Setting", "Description" :widths: 50, 100 :file: tables/table6_aedxd_settings.csv If you want to repeat measurement, you can set 'Iterations' = 2 or higher. .. important:: Confirm the following: - 'Camera Vpos' = 110, 'Beamstop' = OUT, 'Tip X' = 0 - 'Scan1 MCA Trigger Toggle' = OFF (nothing in line 2) Both 'Preset Real Time' and 'Preset Live Time' = 0 - Slit and Filter setup is 'EDXD' condition ('Filter' = 0, slit size is small) 'position of sample is correct'. Then, in :ref:`hpMCA`: #. Make sure file number is set to auto-increment #. Open \ :menuselection:`File --> Preferences` #. In preferences, please check 'yes' for 'autosave when acquisition stopped'. (hpMCA will save file for each angle data with the name suffix of '_001', '_002'...). Then, to start multiangle measurement, - On Multiangle control window, click :guilabel:`Run` .. important:: After finishing the Multiangle collection, please do not forget to check 'no' for 'autosave when acquisition stopped'. If you want to stop the Multiangle measurement, click :guilabel:`Stop`.