16-BM-B PE Press Experiments User Manual

Beamline Overview:

• Beamline description
  • Summary of 16-BM-B features

Sammple Assemblies

• PEC sample assembiles
  • Types of cells
  • Capsule materials

Beamline Operation

• Login
• Start PEC EPICS/MEDM user interface
• EDXD and radiography mode switching
• Radiography measurement
• EDXD measurement
• Bluediamond
• Sample Y and/or Z positions search
  • By radiography image
  • By absorption scan
• Sample X position scan
• Pressure control
  • Compression
  • Decompression
  • PE Press Live valve
• Sample Loading Procedure
• Sample Removal Procedure
  • Sample Removal
• Heating control
• Liquid/amorphous structure measurement
• Ultrasound measurement
• General data logging
• Logging data with Strip Chart
• Hutch webcam
• Data transfer
  • Data transfer tips

Troubleshooting

• Troubleshoot

Beamline Support

• Beamline support
  • Beamline scientist contacts

Beamline software:

• hpMCA
  • GUI basics
  • Acquisition
  • Elapsed time
  • Save data file
  • File saving options
  • Regions of Interest (ROI)
  • Fluorescence markers
  • Vertical scale
  • Horizontal scale
  • Energy calibration
  • 2\({\theta}\) angle calibration